1,2,3,4-Tetra-O-acetyl-beta-D-glucopyranuronic acid monohydrate at 120 K and anhydrous 1,2,3,4-tetra-O-acetyl-beta-D-glucopyranose at 292 K

T C  Baddeley; R A  Howie; J M S  Skakle; J L  Wardell

doi:10.1107/S0108270105034979

1,2,3,4-Tetra-O-acetyl-beta-D-glucopyranuronic acid monohydrate at 120 K and anhydrous 1,2,3,4-tetra-O-acetyl-beta-D-glucopyranose at 292 K

T C Baddeley, R A Howie, J M S Skakle, J L Wardell

Research output: Contribution to journal › Article › peer-review

4 Citations (Scopus)

Abstract

The structure of the title acid as the monohydrate, C(14)H(18)O(11)center dot H2O, displays hydrogen bonding which connects the molecules in layers parallel to (10 (1) over bar). In the anhydrous glucopyranose, C14H20O10, only chain connectivity is attained but, due to disorder of the OH group, only partially and in two modes, one less favoured than the other. This provides incomplete connectivity between molecules in corrugated layers parallel to (010).

Original language	English
Pages (from-to)	o711-o714
Number of pages	4
Journal	Acta Crystallographica Section C, Crystal Structure Communications
Volume	61
Issue number	12
DOIs	https://doi.org/10.1107/S0108270105034979
Publication status	Published - Oct 2005

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1,2,3,4-Tetra-O-acetyl-beta-D-glucopyranuronic acid monohydrate at 120 K and anhydrous 1,2,3,4-tetra-O-acetyl-beta-D-glucopyranose at 292 K. / Baddeley, T C ; Howie, R A ; Skakle, J M S et al.
In: Acta Crystallographica Section C, Crystal Structure Communications, Vol. 61, No. 12, 10.2005, p. o711-o714.

Research output: Contribution to journal › Article › peer-review

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title = "1,2,3,4-Tetra-O-acetyl-beta-D-glucopyranuronic acid monohydrate at 120 K and anhydrous 1,2,3,4-tetra-O-acetyl-beta-D-glucopyranose at 292 K",

abstract = "The structure of the title acid as the monohydrate, C(14)H(18)O(11)center dot H2O, displays hydrogen bonding which connects the molecules in layers parallel to (10 (1) over bar). In the anhydrous glucopyranose, C14H20O10, only chain connectivity is attained but, due to disorder of the OH group, only partially and in two modes, one less favoured than the other. This provides incomplete connectivity between molecules in corrugated layers parallel to (010).",

author = "Baddeley, {T C} and Howie, {R A} and Skakle, {J M S} and Wardell, {J L}",

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T1 - 1,2,3,4-Tetra-O-acetyl-beta-D-glucopyranuronic acid monohydrate at 120 K and anhydrous 1,2,3,4-tetra-O-acetyl-beta-D-glucopyranose at 292 K

AU - Baddeley, T C

AU - Howie, R A

AU - Skakle, J M S

AU - Wardell, J L

PY - 2005/10

Y1 - 2005/10

N2 - The structure of the title acid as the monohydrate, C(14)H(18)O(11)center dot H2O, displays hydrogen bonding which connects the molecules in layers parallel to (10 (1) over bar). In the anhydrous glucopyranose, C14H20O10, only chain connectivity is attained but, due to disorder of the OH group, only partially and in two modes, one less favoured than the other. This provides incomplete connectivity between molecules in corrugated layers parallel to (010).

AB - The structure of the title acid as the monohydrate, C(14)H(18)O(11)center dot H2O, displays hydrogen bonding which connects the molecules in layers parallel to (10 (1) over bar). In the anhydrous glucopyranose, C14H20O10, only chain connectivity is attained but, due to disorder of the OH group, only partially and in two modes, one less favoured than the other. This provides incomplete connectivity between molecules in corrugated layers parallel to (010).

U2 - 10.1107/S0108270105034979

DO - 10.1107/S0108270105034979

M3 - Article

SN - 0108-2701

VL - 61

SP - o711-o714

JO - Acta Crystallographica Section C, Crystal Structure Communications

JF - Acta Crystallographica Section C, Crystal Structure Communications

IS - 12

ER -

1,2,3,4-Tetra-O-acetyl-beta-D-glucopyranuronic acid monohydrate at 120 K and anhydrous 1,2,3,4-tetra-O-acetyl-beta-D-glucopyranose at 292 K

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