1,2,3,4-Tetra-O-acetyl-beta-D-glucopyranuronic acid monohydrate at 120 K and anhydrous 1,2,3,4-tetra-O-acetyl-beta-D-glucopyranose at 292 K

T C Baddeley, R A Howie, J M S Skakle, J L Wardell

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4 Citations (Scopus)

Abstract

The structure of the title acid as the monohydrate, C(14)H(18)O(11)center dot H2O, displays hydrogen bonding which connects the molecules in layers parallel to (10 (1) over bar). In the anhydrous glucopyranose, C14H20O10, only chain connectivity is attained but, due to disorder of the OH group, only partially and in two modes, one less favoured than the other. This provides incomplete connectivity between molecules in corrugated layers parallel to (010).

Original languageEnglish
Pages (from-to)o711-o714
Number of pages4
JournalActa Crystallographica Section C, Crystal Structure Communications
Volume61
Issue number12
DOIs
Publication statusPublished - Oct 2005

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Hydrogen Bonding
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1,2,3,4-tetra-O-acetylglucopyranose

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@article{775e86829bb8421ba25c726d13841e5a,
title = "1,2,3,4-Tetra-O-acetyl-beta-D-glucopyranuronic acid monohydrate at 120 K and anhydrous 1,2,3,4-tetra-O-acetyl-beta-D-glucopyranose at 292 K",
abstract = "The structure of the title acid as the monohydrate, C(14)H(18)O(11)center dot H2O, displays hydrogen bonding which connects the molecules in layers parallel to (10 (1) over bar). In the anhydrous glucopyranose, C14H20O10, only chain connectivity is attained but, due to disorder of the OH group, only partially and in two modes, one less favoured than the other. This provides incomplete connectivity between molecules in corrugated layers parallel to (010).",
author = "Baddeley, {T C} and Howie, {R A} and Skakle, {J M S} and Wardell, {J L}",
year = "2005",
month = "10",
doi = "10.1107/S0108270105034979",
language = "English",
volume = "61",
pages = "o711--o714",
journal = "Acta Crystallographica Section C, Crystal Structure Communications",
issn = "0108-2701",
publisher = "Wiley-Blackwell",
number = "12",

}

TY - JOUR

T1 - 1,2,3,4-Tetra-O-acetyl-beta-D-glucopyranuronic acid monohydrate at 120 K and anhydrous 1,2,3,4-tetra-O-acetyl-beta-D-glucopyranose at 292 K

AU - Baddeley, T C

AU - Howie, R A

AU - Skakle, J M S

AU - Wardell, J L

PY - 2005/10

Y1 - 2005/10

N2 - The structure of the title acid as the monohydrate, C(14)H(18)O(11)center dot H2O, displays hydrogen bonding which connects the molecules in layers parallel to (10 (1) over bar). In the anhydrous glucopyranose, C14H20O10, only chain connectivity is attained but, due to disorder of the OH group, only partially and in two modes, one less favoured than the other. This provides incomplete connectivity between molecules in corrugated layers parallel to (010).

AB - The structure of the title acid as the monohydrate, C(14)H(18)O(11)center dot H2O, displays hydrogen bonding which connects the molecules in layers parallel to (10 (1) over bar). In the anhydrous glucopyranose, C14H20O10, only chain connectivity is attained but, due to disorder of the OH group, only partially and in two modes, one less favoured than the other. This provides incomplete connectivity between molecules in corrugated layers parallel to (010).

U2 - 10.1107/S0108270105034979

DO - 10.1107/S0108270105034979

M3 - Article

VL - 61

SP - o711-o714

JO - Acta Crystallographica Section C, Crystal Structure Communications

JF - Acta Crystallographica Section C, Crystal Structure Communications

SN - 0108-2701

IS - 12

ER -