(1RS,2RS)-N,N '-Bis(4-nitrophenylmethylene)cyclohexane-1,2-diamine: complex sheets built from C-H center dot center dot center dot O and C-H center dot center dot center dot pi(arene) hydrogen bonds

C Glidewell, J N Low, J M S Skakle, J L Wardell

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Abstract

The racemic title compound, C20H20N4O4, crystallizes with Z' = 2 in the space group P2(1)/c. Each independent molecule exhibits approximate twofold rotation symmetry, but conformational differences between the molecules preclude any higher symmetry. The molecules are linked into complex sheets by a combination of four C-H center dot center dot center dot O hydrogen bonds and two C-H center dot center dot center dot pi(arene) hydrogen bonds.

Original languageEnglish
Pages (from-to)o551-o554
Number of pages4
JournalActa Crystallographica Section C, Crystal Structure Communications
Volume61
Issue number9
DOIs
Publication statusPublished - Sep 2005

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Hydrogen
Hydrogen bonds
Molecules
1,2-cyclohexanediamine

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title = "(1RS,2RS)-N,N '-Bis(4-nitrophenylmethylene)cyclohexane-1,2-diamine: complex sheets built from C-H center dot center dot center dot O and C-H center dot center dot center dot pi(arene) hydrogen bonds",
abstract = "The racemic title compound, C20H20N4O4, crystallizes with Z' = 2 in the space group P2(1)/c. Each independent molecule exhibits approximate twofold rotation symmetry, but conformational differences between the molecules preclude any higher symmetry. The molecules are linked into complex sheets by a combination of four C-H center dot center dot center dot O hydrogen bonds and two C-H center dot center dot center dot pi(arene) hydrogen bonds.",
author = "C Glidewell and Low, {J N} and Skakle, {J M S} and Wardell, {J L}",
year = "2005",
month = "9",
doi = "10.1107/S0108270105024443",
language = "English",
volume = "61",
pages = "o551--o554",
journal = "Acta Crystallographica Section C, Crystal Structure Communications",
issn = "0108-2701",
publisher = "Wiley-Blackwell",
number = "9",

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T1 - (1RS,2RS)-N,N '-Bis(4-nitrophenylmethylene)cyclohexane-1,2-diamine

T2 - complex sheets built from C-H center dot center dot center dot O and C-H center dot center dot center dot pi(arene) hydrogen bonds

AU - Glidewell, C

AU - Low, J N

AU - Skakle, J M S

AU - Wardell, J L

PY - 2005/9

Y1 - 2005/9

N2 - The racemic title compound, C20H20N4O4, crystallizes with Z' = 2 in the space group P2(1)/c. Each independent molecule exhibits approximate twofold rotation symmetry, but conformational differences between the molecules preclude any higher symmetry. The molecules are linked into complex sheets by a combination of four C-H center dot center dot center dot O hydrogen bonds and two C-H center dot center dot center dot pi(arene) hydrogen bonds.

AB - The racemic title compound, C20H20N4O4, crystallizes with Z' = 2 in the space group P2(1)/c. Each independent molecule exhibits approximate twofold rotation symmetry, but conformational differences between the molecules preclude any higher symmetry. The molecules are linked into complex sheets by a combination of four C-H center dot center dot center dot O hydrogen bonds and two C-H center dot center dot center dot pi(arene) hydrogen bonds.

U2 - 10.1107/S0108270105024443

DO - 10.1107/S0108270105024443

M3 - Article

VL - 61

SP - o551-o554

JO - Acta Crystallographica Section C, Crystal Structure Communications

JF - Acta Crystallographica Section C, Crystal Structure Communications

SN - 0108-2701

IS - 9

ER -