2-(4-Iodo-1-methyl-1H-pyrazol-3-yl)pyridinium dichloroiodide

Research output: Contribution to journalArticle

Abstract

In the title molecular salt, C9 H9 IN3 + ICl2-, the dihedral angle between the aromatic rings in the cation is 14.9 (2) degrees. The I—Cl bond lengths of the anion are distinctly different, by 0.149 (2) A°. The most significant interaction in the crystal
structure is a bifurcated N—H center dot center dot center dot (N,Cl) hydrogen bond.
Original languageEnglish
Article numbero4045
Number of pages9
JournalActa Crystallographica Section E: Structure Reports Online
Volume63
Issue number10
DOIs
Publication statusPublished - Oct 2007

Cite this

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title = "2-(4-Iodo-1-methyl-1H-pyrazol-3-yl)pyridinium dichloroiodide",
abstract = "In the title molecular salt, C9 H9 IN3 + ICl2-, the dihedral angle between the aromatic rings in the cation is 14.9 (2) degrees. The I—Cl bond lengths of the anion are distinctly different, by 0.149 (2) A°. The most significant interaction in the crystalstructure is a bifurcated N—H center dot center dot center dot (N,Cl) hydrogen bond.",
author = "Harrison, {William T. A.}",
year = "2007",
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doi = "10.1107/S1600536807044169",
language = "English",
volume = "63",
journal = "Acta Crystallographica Section E: Structure Reports Online",
issn = "1600-5368",
publisher = "International Union of Crystallography",
number = "10",

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T1 - 2-(4-Iodo-1-methyl-1H-pyrazol-3-yl)pyridinium dichloroiodide

AU - Harrison, William T. A.

PY - 2007/10

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N2 - In the title molecular salt, C9 H9 IN3 + ICl2-, the dihedral angle between the aromatic rings in the cation is 14.9 (2) degrees. The I—Cl bond lengths of the anion are distinctly different, by 0.149 (2) A°. The most significant interaction in the crystalstructure is a bifurcated N—H center dot center dot center dot (N,Cl) hydrogen bond.

AB - In the title molecular salt, C9 H9 IN3 + ICl2-, the dihedral angle between the aromatic rings in the cation is 14.9 (2) degrees. The I—Cl bond lengths of the anion are distinctly different, by 0.149 (2) A°. The most significant interaction in the crystalstructure is a bifurcated N—H center dot center dot center dot (N,Cl) hydrogen bond.

U2 - 10.1107/S1600536807044169

DO - 10.1107/S1600536807044169

M3 - Article

VL - 63

JO - Acta Crystallographica Section E: Structure Reports Online

JF - Acta Crystallographica Section E: Structure Reports Online

SN - 1600-5368

IS - 10

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ER -