Bilayers in 4-iodo-N-(2-iodo-4-nitrophenyl)benzamide generated by a combination of an N-H...O=C hydrogen bond and two independent iodo...nitro interactions

C. Glidewell, J. L. Wardell, Janet Mabel Scott Skakle

Research output: Contribution to journalArticle

5 Citations (Scopus)

Abstract

Molecules of the title compound, C13H8I2N2O3, are linked into C(4) chains by a single N-H...O=C hydrogen bond [H...O = 2.10 Angstrom, N...O = 2.832(5) Angstrom and N-H...O = 140degrees]. Two independent two-centre iodo-nitro interactions, both involving the same O atom but different I atoms [I...O = 3.205 (3) and 3.400 (3) Angstrom, and C-I...O = 160.4 (2) and 155.7 (2)degrees], link the hydrogen-bonded chains into bilayers.

Original languageEnglish
Pages (from-to)o636-o637
Number of pages2
JournalActa Crystallographica Section C, Crystal Structure Communications
VolumeC59
DOIs
Publication statusPublished - 2003

Keywords

  • PI-STACKING INTERACTIONS
  • INTERPLAY
  • PATTERNS

Cite this

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title = "Bilayers in 4-iodo-N-(2-iodo-4-nitrophenyl)benzamide generated by a combination of an N-H...O=C hydrogen bond and two independent iodo...nitro interactions",
abstract = "Molecules of the title compound, C13H8I2N2O3, are linked into C(4) chains by a single N-H...O=C hydrogen bond [H...O = 2.10 Angstrom, N...O = 2.832(5) Angstrom and N-H...O = 140degrees]. Two independent two-centre iodo-nitro interactions, both involving the same O atom but different I atoms [I...O = 3.205 (3) and 3.400 (3) Angstrom, and C-I...O = 160.4 (2) and 155.7 (2)degrees], link the hydrogen-bonded chains into bilayers.",
keywords = "PI-STACKING INTERACTIONS, INTERPLAY, PATTERNS",
author = "C. Glidewell and Wardell, {J. L.} and Skakle, {Janet Mabel Scott}",
year = "2003",
doi = "10.1107/S0108270103021164",
language = "English",
volume = "C59",
pages = "o636--o637",
journal = "Acta Crystallographica Section C, Crystal Structure Communications",
issn = "0108-2701",
publisher = "Wiley-Blackwell",

}

TY - JOUR

T1 - Bilayers in 4-iodo-N-(2-iodo-4-nitrophenyl)benzamide generated by a combination of an N-H...O=C hydrogen bond and two independent iodo...nitro interactions

AU - Glidewell, C.

AU - Wardell, J. L.

AU - Skakle, Janet Mabel Scott

PY - 2003

Y1 - 2003

N2 - Molecules of the title compound, C13H8I2N2O3, are linked into C(4) chains by a single N-H...O=C hydrogen bond [H...O = 2.10 Angstrom, N...O = 2.832(5) Angstrom and N-H...O = 140degrees]. Two independent two-centre iodo-nitro interactions, both involving the same O atom but different I atoms [I...O = 3.205 (3) and 3.400 (3) Angstrom, and C-I...O = 160.4 (2) and 155.7 (2)degrees], link the hydrogen-bonded chains into bilayers.

AB - Molecules of the title compound, C13H8I2N2O3, are linked into C(4) chains by a single N-H...O=C hydrogen bond [H...O = 2.10 Angstrom, N...O = 2.832(5) Angstrom and N-H...O = 140degrees]. Two independent two-centre iodo-nitro interactions, both involving the same O atom but different I atoms [I...O = 3.205 (3) and 3.400 (3) Angstrom, and C-I...O = 160.4 (2) and 155.7 (2)degrees], link the hydrogen-bonded chains into bilayers.

KW - PI-STACKING INTERACTIONS

KW - INTERPLAY

KW - PATTERNS

U2 - 10.1107/S0108270103021164

DO - 10.1107/S0108270103021164

M3 - Article

VL - C59

SP - o636-o637

JO - Acta Crystallographica Section C, Crystal Structure Communications

JF - Acta Crystallographica Section C, Crystal Structure Communications

SN - 0108-2701

ER -