N,N′-Bis(3-methylbut-2-enyl)-N,N′-(1,4-phenylene) dibenzenesulfonamide

null Ejaz; Islam Ullah Khan; Tahir Ali Sheikh; William T A Harrison

doi:10.1107/S1600536811045661

N,N′-Bis(3-methylbut-2-enyl)-N,N′-(1,4-phenylene) dibenzenesulfonamide

Ejaz, Islam Ullah Khan^*, Tahir Ali Sheikh, William T A Harrison

^*Corresponding author for this work

Chemistry

Government College University Lahore

Research output: Contribution to journal › Article › peer-review

Abstract

The complete molecule of the title compound, C₂₈H ₃₂N₂O₄S₂, is generated by a crystallographic inversion centre. The dihedral angle between the central and pendant aromatic rings is 46.78 (7)°. The C_ar-S-N-C_ar (ar = aromatic) torsion angle is 73.64 (15)°and the bond-angle sum for the N atom is 350.4°. In the crystal, weak C-H⋯O interactions link the molecules, forming a two-dimensional network lying parallel to the bc plane.

Original language	English
Journal	Acta Crystallographica Section E: Structure Reports Online
Volume	67
Issue number	12
DOIs	https://doi.org/10.1107/S1600536811045661
Publication status	Published - 1 Dec 2011

Keywords

crystal X-ray study
data-to-parameter ratio = 16.2
mean σ(C-C) = 0.003 Å
R factor = 0.039
T = 296 K
wR factor = 0.104

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title = "N,N′-Bis(3-methylbut-2-enyl)-N,N′-(1,4-phenylene) dibenzenesulfonamide",

abstract = "The complete molecule of the title compound, C28H 32N2O4S2, is generated by a crystallographic inversion centre. The dihedral angle between the central and pendant aromatic rings is 46.78 (7)°. The Car-S-N-Car (ar = aromatic) torsion angle is 73.64 (15)°and the bond-angle sum for the N atom is 350.4°. In the crystal, weak C-H⋯O interactions link the molecules, forming a two-dimensional network lying parallel to the bc plane.",

keywords = "crystal X-ray study, data-to-parameter ratio = 16.2, mean σ(C-C) = 0.003 {\AA}, R factor = 0.039, T = 296 K, wR factor = 0.104",

author = "Ejaz and Khan, {Islam Ullah} and Sheikh, {Tahir Ali} and Harrison, {William T A}",

year = "2011",

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doi = "10.1107/S1600536811045661",

language = "English",

volume = "67",

journal = "Acta Crystallographica Section E: Structure Reports Online",

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TY - JOUR

T1 - N,N′-Bis(3-methylbut-2-enyl)-N,N′-(1,4-phenylene) dibenzenesulfonamide

AU - Ejaz, null

AU - Khan, Islam Ullah

AU - Sheikh, Tahir Ali

AU - Harrison, William T A

PY - 2011/12/1

Y1 - 2011/12/1

N2 - The complete molecule of the title compound, C28H 32N2O4S2, is generated by a crystallographic inversion centre. The dihedral angle between the central and pendant aromatic rings is 46.78 (7)°. The Car-S-N-Car (ar = aromatic) torsion angle is 73.64 (15)°and the bond-angle sum for the N atom is 350.4°. In the crystal, weak C-H⋯O interactions link the molecules, forming a two-dimensional network lying parallel to the bc plane.

AB - The complete molecule of the title compound, C28H 32N2O4S2, is generated by a crystallographic inversion centre. The dihedral angle between the central and pendant aromatic rings is 46.78 (7)°. The Car-S-N-Car (ar = aromatic) torsion angle is 73.64 (15)°and the bond-angle sum for the N atom is 350.4°. In the crystal, weak C-H⋯O interactions link the molecules, forming a two-dimensional network lying parallel to the bc plane.

KW - crystal X-ray study

KW - data-to-parameter ratio = 16.2

KW - mean σ(C-C) = 0.003 Å

KW - R factor = 0.039

KW - T = 296 K

KW - wR factor = 0.104

UR - http://www.scopus.com/inward/record.url?scp=83155178467&partnerID=8YFLogxK

U2 - 10.1107/S1600536811045661

DO - 10.1107/S1600536811045661

M3 - Article

AN - SCOPUS:83155178467

SN - 1600-5368

VL - 67

JO - Acta Crystallographica Section E: Structure Reports Online

JF - Acta Crystallographica Section E: Structure Reports Online

IS - 12

ER -

N,N′-Bis(3-methylbut-2-enyl)-N,N′-(1,4-phenylene) dibenzenesulfonamide

Abstract

Keywords

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