The influence of pulsed laser powder bed fusion process parameters on Inconel 718 material properties

Konstantinos Georgilas* (Corresponding Author), Raja H.U. Khan, Mehmet E. Kartal

*Corresponding author for this work

Research output: Contribution to journalArticle

Abstract

In this work, the effect of pulsed laser used during the powder bed fusion (L-PBF) additive manufacturing (AM) process on Inconel 718 (IN718) material properties has been investigated. Argon gas atomised (AGA) IN718 powder is characterised in terms of flow, density, particle size distribution and morphology. Powder shows mostly spherical morphology with Hausner ratio of 1.17 indicating good flow characteristics. Density optimisation trials are carried out by varying laser power and exposure time. Fabricated samples are characterised in terms of porosity by area fraction analysis using light microscopy and volume fraction analysis using X-ray microcomputed tomography (micro-CT). Minimum porosity of 0.16% is achieved for laser power of 200 W and exposure time of 110 μs＀ Microstructural analysis using the Electron Backscatter Diffraction (EBSD) technique shows limited columnar grain structure in the Z direction and more equiaxed type grains in the XY direction (normal to the Z direction). Tensile test results show 754 MPa yield strength, 1070 MPa ultimate tensile strength and ~24% elongation. Finally, hole drilling residual stress measurements show increase from ~0 MPa to over 450 MPa in tensile stress up to a depth of 1 mm from the top surface of the as-build L-PBF IN718 sample. It has been found that laser pulsing produces higher homogeneity in grain structure and better mechanical properties than that by the continuous laser method.
Original languageEnglish
Article number138527
Number of pages9
JournalMaterials Science and Engineering A
Volume769
Early online date9 Oct 2019
DOIs
Publication statusE-pub ahead of print - 9 Oct 2019

Fingerprint

Inconel (trademark)
Pulsed lasers
Powders
beds
pulsed lasers
Materials properties
Fusion reactions
fusion
Lasers
Crystal microstructure
lasers
3D printers
Porosity
porosity
stress measurement
Argon
Stress measurement
flow characteristics
X ray analysis
yield strength

Keywords

  • Powder methods
  • Nickel alloys
  • Grains and interfaces
  • Stress/strain measurements
  • Characterisation

Cite this

The influence of pulsed laser powder bed fusion process parameters on Inconel 718 material properties. / Georgilas, Konstantinos (Corresponding Author); Khan, Raja H.U.; Kartal, Mehmet E.

In: Materials Science and Engineering A, Vol. 769, 138527, 02.01.2020.

Research output: Contribution to journalArticle

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abstract = "In this work, the effect of pulsed laser used during the powder bed fusion (L-PBF) additive manufacturing (AM) process on Inconel 718 (IN718) material properties has been investigated. Argon gas atomised (AGA) IN718 powder is characterised in terms of flow, density, particle size distribution and morphology. Powder shows mostly spherical morphology with Hausner ratio of 1.17 indicating good flow characteristics. Density optimisation trials are carried out by varying laser power and exposure time. Fabricated samples are characterised in terms of porosity by area fraction analysis using light microscopy and volume fraction analysis using X-ray microcomputed tomography (micro-CT). Minimum porosity of 0.16{\%} is achieved for laser power of 200 W and exposure time of 110 μs＀ Microstructural analysis using the Electron Backscatter Diffraction (EBSD) technique shows limited columnar grain structure in the Z direction and more equiaxed type grains in the XY direction (normal to the Z direction). Tensile test results show 754 MPa yield strength, 1070 MPa ultimate tensile strength and ~24{\%} elongation. Finally, hole drilling residual stress measurements show increase from ~0 MPa to over 450 MPa in tensile stress up to a depth of 1 mm from the top surface of the as-build L-PBF IN718 sample. It has been found that laser pulsing produces higher homogeneity in grain structure and better mechanical properties than that by the continuous laser method.",
keywords = "Powder methods, Nickel alloys, Grains and interfaces, Stress/strain measurements, Characterisation",
author = "Konstantinos Georgilas and Khan, {Raja H.U.} and Kartal, {Mehmet E.}",
note = "Funding This publication was made possible by the sponsorship and support of Lloyd's Register Foundation, United Kingdom. The work was enabled through, and undertaken at, the National Structural Integrity Research Centre (NSIRC) United Kingdom, a postgraduate engineering facility for industry-led research into structural integrity established and managed by TWI through a network of both national and international Universities. Lloyd’s Register Foundation helps to protect life and property by supporting engineering-related education, public engagement and the application of research. Data availability The raw data required to reproduce these findings cannot be shared at this time as the data also forms part of an ongoing study. The processed data required to reproduce these findings cannot be shared at this time as the data also forms part of an ongoing study.",
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N2 - In this work, the effect of pulsed laser used during the powder bed fusion (L-PBF) additive manufacturing (AM) process on Inconel 718 (IN718) material properties has been investigated. Argon gas atomised (AGA) IN718 powder is characterised in terms of flow, density, particle size distribution and morphology. Powder shows mostly spherical morphology with Hausner ratio of 1.17 indicating good flow characteristics. Density optimisation trials are carried out by varying laser power and exposure time. Fabricated samples are characterised in terms of porosity by area fraction analysis using light microscopy and volume fraction analysis using X-ray microcomputed tomography (micro-CT). Minimum porosity of 0.16% is achieved for laser power of 200 W and exposure time of 110 μs＀ Microstructural analysis using the Electron Backscatter Diffraction (EBSD) technique shows limited columnar grain structure in the Z direction and more equiaxed type grains in the XY direction (normal to the Z direction). Tensile test results show 754 MPa yield strength, 1070 MPa ultimate tensile strength and ~24% elongation. Finally, hole drilling residual stress measurements show increase from ~0 MPa to over 450 MPa in tensile stress up to a depth of 1 mm from the top surface of the as-build L-PBF IN718 sample. It has been found that laser pulsing produces higher homogeneity in grain structure and better mechanical properties than that by the continuous laser method.

AB - In this work, the effect of pulsed laser used during the powder bed fusion (L-PBF) additive manufacturing (AM) process on Inconel 718 (IN718) material properties has been investigated. Argon gas atomised (AGA) IN718 powder is characterised in terms of flow, density, particle size distribution and morphology. Powder shows mostly spherical morphology with Hausner ratio of 1.17 indicating good flow characteristics. Density optimisation trials are carried out by varying laser power and exposure time. Fabricated samples are characterised in terms of porosity by area fraction analysis using light microscopy and volume fraction analysis using X-ray microcomputed tomography (micro-CT). Minimum porosity of 0.16% is achieved for laser power of 200 W and exposure time of 110 μs＀ Microstructural analysis using the Electron Backscatter Diffraction (EBSD) technique shows limited columnar grain structure in the Z direction and more equiaxed type grains in the XY direction (normal to the Z direction). Tensile test results show 754 MPa yield strength, 1070 MPa ultimate tensile strength and ~24% elongation. Finally, hole drilling residual stress measurements show increase from ~0 MPa to over 450 MPa in tensile stress up to a depth of 1 mm from the top surface of the as-build L-PBF IN718 sample. It has been found that laser pulsing produces higher homogeneity in grain structure and better mechanical properties than that by the continuous laser method.

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