Racemic cis-methoxobis(2-methyl-2-oxo-4H-pyran-4-olato)oxovanadium(V) redetermined at 120 K: hydrogen-bonded ribbons containing R (7), R (14) and R (18) rings

S. J. Kavitha, K. Panchanatheswaran, C. Glidewell

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    Abstract

    In the title compound, [V(CH3O)(C6H5O3)(2)O], the V - O bond lengths to the oxo and methoxo ligands are 1.593 ( 3) and 1.768 (3) angstrom, respectively, at 120 K; the V - O bond lengths trans to these two ligands are 2.246 ( 3) and 2.116 ( 3) angstrom. Molecules are linked by three C - H center dot center dot center dot O hydrogen bonds into complex ribbons containing three types of ring.

    Original languageEnglish
    Pages (from-to)M116-M118
    Number of pages3
    JournalActa Crystallographica Section C, Crystal Structure Communications
    Volume62
    Issue number62
    DOIs
    Publication statusPublished - 2006

    Keywords

    • X-RAY
    • BIS(MALTOLATO)OXOVANADIUM(IV)
    • DIFFRACTION
    • COMPLEXES

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