Three-dimensional in situ observations of compressive damage mechanisms in syntactic foam using X-ray microcomputed tomography

M E Kartal, L H Dugdale, J J Harrigan, M A Siddiq, D Pokrajac, D M Mulvihill

Research output: Contribution to journalArticle

4 Citations (Scopus)
5 Downloads (Pure)

Abstract

Syntactic foams with hollow glass microspheres embedded in an epoxy matrix are used in marine, aerospace and ground transportation vehicle applications. This work presents an in situ experimental study of failure mechanisms in syntactic foam based on X-ray microcomputed tomography with uniaxial compression. Under different levels of compressive strain, the material was scanned using X-ray microcomputed tomography to obtain three-dimensional (3D) images of its internal microstructure. Experiments with the same parameters were carried out to investigate repeatability. The microscopic observations have suggested that damage nucleation occurs at the weakest microspheres. When applied strain increases, shear collapse bands (SCBs) develop local to the fragmented microspheres due to stress concentration and bending deformation around SCBs occurs. After significant strain, the thickness of the SCBs increases owing to the accumulation of the broken microspheres. The relationship between the volume fraction of microspheres and applied bulk strain has been characterised.
Original languageEnglish
Pages (from-to)10186-10197
Number of pages11
JournalJournal of Materials Science
Volume52
Issue number17
Early online date31 May 2017
DOIs
Publication statusPublished - Sep 2017

Fingerprint

Syntactics
Microspheres
Tomography
Foams
Shear bands
X rays
Bending (deformation)
Stress concentration
Volume fraction
Nucleation
Glass
Microstructure
Experiments

Keywords

  • syntactic foams
  • damage mechanisms
  • X-Ray micro-computed tomography
  • microstructure
  • compression

Cite this

Three-dimensional in situ observations of compressive damage mechanisms in syntactic foam using X-ray microcomputed tomography. / Kartal, M E; Dugdale, L H; Harrigan, J J ; Siddiq, M A; Pokrajac, D; Mulvihill, D M.

In: Journal of Materials Science, Vol. 52, No. 17, 09.2017, p. 10186-10197.

Research output: Contribution to journalArticle

@article{dc1fd52727ad435ab625c2685dbc9d43,
title = "Three-dimensional in situ observations of compressive damage mechanisms in syntactic foam using X-ray microcomputed tomography",
abstract = "Syntactic foams with hollow glass microspheres embedded in an epoxy matrix are used in marine, aerospace and ground transportation vehicle applications. This work presents an in situ experimental study of failure mechanisms in syntactic foam based on X-ray microcomputed tomography with uniaxial compression. Under different levels of compressive strain, the material was scanned using X-ray microcomputed tomography to obtain three-dimensional (3D) images of its internal microstructure. Experiments with the same parameters were carried out to investigate repeatability. The microscopic observations have suggested that damage nucleation occurs at the weakest microspheres. When applied strain increases, shear collapse bands (SCBs) develop local to the fragmented microspheres due to stress concentration and bending deformation around SCBs occurs. After significant strain, the thickness of the SCBs increases owing to the accumulation of the broken microspheres. The relationship between the volume fraction of microspheres and applied bulk strain has been characterised.",
keywords = "syntactic foams, damage mechanisms, X-Ray micro-computed tomography, microstructure, compression",
author = "Kartal, {M E} and Dugdale, {L H} and Harrigan, {J J} and Siddiq, {M A} and D Pokrajac and Mulvihill, {D M}",
note = "Royal Society Grant number RG140680 Lloyd's Register Foundation (GB) Oil and Gas Academy of Scotland Open access via Springer Compact Agreement",
year = "2017",
month = "9",
doi = "10.1007/s10853-017-1177-4",
language = "English",
volume = "52",
pages = "10186--10197",
journal = "Journal of Materials Science",
issn = "0022-2461",
publisher = "Springer Netherlands",
number = "17",

}

TY - JOUR

T1 - Three-dimensional in situ observations of compressive damage mechanisms in syntactic foam using X-ray microcomputed tomography

AU - Kartal, M E

AU - Dugdale, L H

AU - Harrigan, J J

AU - Siddiq, M A

AU - Pokrajac, D

AU - Mulvihill, D M

N1 - Royal Society Grant number RG140680 Lloyd's Register Foundation (GB) Oil and Gas Academy of Scotland Open access via Springer Compact Agreement

PY - 2017/9

Y1 - 2017/9

N2 - Syntactic foams with hollow glass microspheres embedded in an epoxy matrix are used in marine, aerospace and ground transportation vehicle applications. This work presents an in situ experimental study of failure mechanisms in syntactic foam based on X-ray microcomputed tomography with uniaxial compression. Under different levels of compressive strain, the material was scanned using X-ray microcomputed tomography to obtain three-dimensional (3D) images of its internal microstructure. Experiments with the same parameters were carried out to investigate repeatability. The microscopic observations have suggested that damage nucleation occurs at the weakest microspheres. When applied strain increases, shear collapse bands (SCBs) develop local to the fragmented microspheres due to stress concentration and bending deformation around SCBs occurs. After significant strain, the thickness of the SCBs increases owing to the accumulation of the broken microspheres. The relationship between the volume fraction of microspheres and applied bulk strain has been characterised.

AB - Syntactic foams with hollow glass microspheres embedded in an epoxy matrix are used in marine, aerospace and ground transportation vehicle applications. This work presents an in situ experimental study of failure mechanisms in syntactic foam based on X-ray microcomputed tomography with uniaxial compression. Under different levels of compressive strain, the material was scanned using X-ray microcomputed tomography to obtain three-dimensional (3D) images of its internal microstructure. Experiments with the same parameters were carried out to investigate repeatability. The microscopic observations have suggested that damage nucleation occurs at the weakest microspheres. When applied strain increases, shear collapse bands (SCBs) develop local to the fragmented microspheres due to stress concentration and bending deformation around SCBs occurs. After significant strain, the thickness of the SCBs increases owing to the accumulation of the broken microspheres. The relationship between the volume fraction of microspheres and applied bulk strain has been characterised.

KW - syntactic foams

KW - damage mechanisms

KW - X-Ray micro-computed tomography

KW - microstructure

KW - compression

U2 - 10.1007/s10853-017-1177-4

DO - 10.1007/s10853-017-1177-4

M3 - Article

VL - 52

SP - 10186

EP - 10197

JO - Journal of Materials Science

JF - Journal of Materials Science

SN - 0022-2461

IS - 17

ER -